Synthesis Position and Optical Properties of BODIPY with Active Group on meso-Position

статья
Авторы публикации: 
Gruzdev M. , Chervonova U. , BumaginaN. , Kolker A.
Журнал: 
Letters in Organic Chemistry
Год публикации: 
2016
Том/страницы: 
V 13, № 10. -- P. 718-725.

IR spectra were recorded on a Bruker Vertex 80V device in the regions of 7500-350 cm(-1) from pellets with KBr. The NMR spectral studies on the nuclei 1H and C-13 were performed on a Bruker Avance-500 instrument (500.13 MHz) in CDC13, the internal standard was TMS. Elemental analyses of crystalline compounds were carried out on a FlashEA 1112 analyzer. Mass spectra were registered on a JMS-700 JEOL (FAB) and JMS-100GCV JEOL (EI) mass-spectrometers. UVN is spectra and fluorescence spectra were recorded on a spectrofluorimeter CM 2203 (SOLAR) in CH2Cl2, with square quartz cavity being 10 mm thick. The fluorescence quantum yield was determined by formula utilizing fluorescein in 0.1 M NaOH as a standard (Phi(s)=0.85).

Опубликовано:
Колкер Аркадий Михайлович
(30.03.2017)